BRUKER APEX III UPGRADE

One ethylene group is disordered over two orientations in a 0.502 (6):0.498 (6) ratio. The Fe atom is displaced by 0.219 (2) A Лљ toward the trifluoromethanesulfonate anion from the 24-atom mean plane of the porphyrin, resulting in a distorted FeN4O square-based pyramidal geometry. Bruker services & support provide you with software downloads of patches and early access modules, service agreements with our One Success program or analytical services that give you early access to latest Bruker technologies. CiteSeerX - Document Details (Isaac Councill, Lee Giles, Pradeep Teregowda): disorder in main residue R factor 0.028 wR factor 0.072 data-to-parameter ratio 11.7. Faster, higher quality diffraction images & data. A Bruker Kappa Apex II CCD diffractometer was used to collect single-crystal data for D 16 Br and its complex with lanthanum(III) nitrate (- and -scan modes, graphite monochromated Mo K 0.71073 Г…) radiation, 150(2) K.

BRUKER APEX III UPGRADE

The title compound,, is an iron(III) porphyrin complex with the trifluoromethanesulfonate anion as an axial ligand. Upgrade to a Bruker PHOTON II Detector to enhance your SC-XRD (D8 QUEST, D8 VENTURE, SMART APEX & KAPPA APEX). 6731 reflections 452 parameters Z =2 Mo K radiation = 0.56 mm 1 T = 100 (2) K 0.52 0.36 0.35 mm 17956 measured reflections 6731 independent reflections 6207 reflections with I>2 (I) Rint = 0.019 26 restraints H-atom parameters constrained max = 1.02 e A Лљ 3 min = 0.65 e A Лљ 3 Key indicators: single-crystal X-ray study T = 100 K mean (CвЂ“C) = 0.003 AЛљ disorder in main residue R factor = 0.038 wR factor = 0.107 data-to-parameter ratio = 14.9.

Bruker apex iii